|
Fatty
Acid Profile
Functional Components
Fatty
Acid Profile
Woodson-Tenent Laboratories, Inc.
345 ADAMS AVE
P O BOX 2135
MEMPHIS TN 38101
(901) 521-4500
SAMPLE NO. : M 98-829584
SAMPLE OF: NOT STATED
SAMPLE ID: CMO SAMPLE BATCH# 0998
PO NUMBER:
CUST #: 01236800
W-T REPORTING DATE: 9/25/98
ENTRY DATE: 9/21/98
REPORT
OF ANALYSIS
|
TEST
RESULT
|
FATTY
ACID PROFILE
|
%
RELATIVE
LISTED BELOW
|
|
C08:0
|
OCTANOIC
(CAPRLYLIC)
|
0.46
%
|
|
C10:0
|
DECANOIC
(CAPRIC)
|
1.86
%
|
|
C11:0
|
UNDECANOIC
(HENDECANOIC)
|
<0.1
%
|
|
C12:0
|
DODECANOIC
(LAURIC)
|
3.14
%
|
|
C14:0
|
TETRADECANOIC
(MYRISTIC)
|
51.3
%
|
|
C14:1
|
TETRADECENOIC
(MYRISTOLEIC)
|
8.23
%
|
|
C15:0
|
PENTADECANOIC
|
2.75
%
|
|
C15:1
|
PENTADECENOIC
|
<0.1
%
|
|
C16:0
|
HEXADECANOIC
(PALMITIC)
|
16.8
%
|
|
C16:1
|
HEXADECENOIC
(PALMATOLEIC)
|
3.32
%
|
|
C16:2
|
HEXADECADIENOIC
|
<0.1
%
|
|
C16:3
|
HEXADECATRIENOIC
|
<0.1
%
|
|
C16:4
|
HEXADECATETRANOIC
|
<0.1
%
|
|
C17:0
|
HEPTADECANOIC
(MARGARIC)
|
0.20
%
|
|
C17:1
|
HEPTADECENOIC
(MARGAROLEIC)
|
0.12
%
|
|
C18:0
|
OCTADECANOIC
(STERIC)
|
3.21
%
|
|
C18:1
|
OCTADECENOIC
(OLEIC)
|
3.28
%
|
|
C18:2
|
OCTADECADIENOIC
(LINOLEIC)
|
0.20
%
|
|
C18:3
|
OCTADECATRIENOIC
(LINOLENIC)
|
<0.1
%
|
|
C18:4
|
OCTADECATETRAENOIC
|
<0.1
%
|
|
C19:0
|
NONDECANOIC
|
<0.1
%
|
|
C20:0
|
EICOSANOIC
(ARACHIDIC)
|
<0.1
%1
|
|
C20:1
|
EICOSENOIC
(GADOLEIC)
|
<0.1
%
|
|
C20:2
|
EICOSADIEONIC
|
<0.1
%
|
|
C20:3
|
EICOSATRIENOIC
|
<0.1
%
|
|
C20:4
|
EICOSATETRAENOIC
(ARACHIDONIC)
|
<0.1
%
|
|
C20:5
|
EICOSAPENTAENOIC
|
<0.1
%
|
|
C21:0
|
HENEICOSANOIC
|
<0.1
%
|
|
C21:5
|
HENEICSAPENTAENOIC
|
<0.1
%
|
|
C22:0
|
DOCOSANOIC
(BEHENIC)
|
<0.1
%
|
|
C22:1
|
DOCOSENOIC
(ERUCIC)
|
<0.1
%
|
|
C22:2
|
DOCOSADIENOIC
|
<0.1
%
|
|
C22:3
|
DOCOSATRIENOIC
|
<0.1
%
|
|
C22:4
|
DOCOSATETRAENOIC
|
<0.1
%
|
|
C22:5
|
DOCOSAPENTAENOIC
|
<0.1
%
|
|
C22:6
|
DOCOSAHEXAENOIC
|
<0.1
%
|
|
C24:0
|
TETRACOSANOIC
|
<0.1
%
|
|
C24:1
|
TETRACOSENOIC
|
<0.1
%
|
|
|
UNKNOWN
COMPONENTS
|
5.13
%
|
RESPECTFULLY
SUBMITTED, WOODSON-TENENT LABORATORIES, INC.
J A WILLIAMS
BRANCH MANAGER
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Components Menu
Functional
Component-Raw Material
Product:
CMO Raw Material (beef tallow extract)
Test Method: Gas Chromatographic (GCFID)
Test Results: See Fatty
Acid Profile sample number M98-829584
Comments: The following information regarding
the functional components of CMO all relate to the fatty acid
profile tests.
Fatty Acid Profile: On 9/25/98, Woodson –
Tenent Laboratories preformed a test on our product sample.
The sample number M98-829584 came from CMO batch number 0998.
Letter: Mr. Casey Rollins of Woodson-Tenent
Laboratories wrote Jim Kniffen of CMO Distribution Centers
a letter on 5/27/99. The letter from Mr. Rollins indicates
the specific methods of analysis used on our CMO product.
Please note the method for Fatty Acid Composition is listed
as AOAC 969.33, which is the Gas Chromatographic Method. (transcript
of letter coming soon)
AOAC Official Methods Of Analysis: This is
a copy of the “Gas Chromatographic Method” this
is the method that is used by Woodson-Tenent Laboratories
to test what is in CMO. (transcript of Gas Chromatographic
Method coming soon) |
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Product
Standard-Raw Material
Product:
CMO Raw Material (beef tallow extract)
Physical Description:
Color: Off-white to Tan
Odor: Faint fatty-acid smell
Texture: Waxy Solid
Melting Point: 50° C (Range 40 – 60° C)
Identification: Mixed ester, alcohol, tallow-acid wax.
Differential Thermal Analysis (DTA):
Minimum between 50-60șC with therogram structure depending
on scan rate and packing sample tube. (associated Graphs &
Summary coming soon)
Infrared Spectrum:
Neat on NaCl plates. (associated Graphs & Summary
coming soon)
Note: The CMO Product Standard is determined by Minitherm
Differential Test Analysis unit vs. alumina reference material
Nujol mull on NaCL plate. The tests are preformed using a
Buck Scientific, Model 500, Infra-red Spectrometer. For more
details see Functional Component test information, DTA Test
Method.
Microbial Testing:
Total Plate Count: <25cfu per gram.
E. Coli:Negative.
Salmonella: Negative.
Functional Component Minimum Fatty Acid Profile, percent relative:
Tetradecanoic (Myristic): >20.0%
Tetradecanoic (Myristoleic): >4.20%
Hexadecenoic (Palmitoleic): >1.25%
Octadecenoic (Oleic): >1.50%
Octadecadienoic (Linoleic): >0.01%
Note: The standards for our beef tallow fatty acid extract
are monitored by GCFID testing. For more details see-“Functional
Component” test information, Gas Chromatographic Test
Methodology. This product is very new. We have improved our
extraction process so that today’s CMO far exceeds our
original standard. |
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Functional
Component Test Methodology-Raw Material
Product:
CMO Raw Material (beef tallow extract)
Tests: Gas Chromatographic (GCFID), Differential Thermal
Analysis (DTA)
Comments: The following describes the methods and
equipment used in testing CMO Raw Materials.
Differential Thermal Analysis (DTA) Test Methodology
In the differential thermal analysis (DTA) technique
the temperature of a sample of reference material, e.g., alumina,
and the temperature of the sample of interest, e.g., CMO wax
are determined as both samples are simultaneously heated up
in a metal block. Although heated at the same rate, the temperatures
of the two samples will differ due to the differences in heat
capacities. A plot of the temperature difference as a function
of the programmed (heating block) temperature indicates transition
temperature (s) and whether the translation is endothermic
or exothermic.
Major Equipment Utilization For Differential Thermal Analysis-CMO
Testing
DTA analysis are conducted using a MINITHERM DTA
unit available from the R.S. Wagner Co., Box 56, Parkesburg,
PA. 19635 (Phone: 610-384-3587).
Gas Chromatographic (GCFID)
Test Methodology
The Gas Chromatographic Method, is described in
AOAC “Official Methods of Analysis”,1990, section
963.22. See Attached AOAC reference. |
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